Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2'-nitrobenzenesulfonyl)-glutamine

Chemical Research in Chinese Universities ›› 2006, Vol. 22 ›› Issue (6): 760-762.doi:

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Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2'-nitrobenzenesulfonyl)-glutamine

XIAO Yong-jun, WANG Jian-guo, WANG Bao-lei, LI Zheng-ming and SONG Hai-bin

Elemento-Organic Chemistry Institute, State Key Laboratory of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China

Received:2005-10-26 Revised:1900-01-01 Online:2006-11-25 Published:2006-11-25
Contact: LI Zheng-ming E-mail:nkzml@nk.sina.net

Abstract

Abstract: The title compound, 5-N-i-propyl-2-(2’-nitrobenzenesulfonyl)-glutamine, was synthesized and its structure was confirmed by IR, MS, ¹H NMR, and elemental analysis. The single crystal structure of the title compound was determined by X-ray diffraction. The crystal belongs to Monoclinic, space group P2(1), with a=0.69281(11) nm, b=0.76508(12), c=1.5843(3) nm, α=90°, β=90.941(3)°, γ=90°, V=0.8397(2) nm³, Z=2, D_c=1.477 g/cm³, μ=0.236 mm^-1, F(000)=392, R=0.0297, and wR=0.0664.

Key words: 5-N-i-Propyl-2-(2-nitrobenzenesulfonyl)-glutamine, Synthesis, Crystal structure

XIAO Yong-jun, WANG Jian-guo, WANG Bao-lei, LI Zheng-ming , SONG Hai-bin. Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2'-nitrobenzenesulfonyl)-glutamine[J]. Chemical Research in Chinese Universities, 2006, 22(6): 760-762.

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Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2'-nitrobenzenesulfonyl)-glutamine

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