Remote Synthesis of Layered Double Hydroxide Nanosheets Through the Automatic Chemical Robot

doi:10.1007/s40242-021-1358-1

Chemical Research in Chinese Universities ›› 2022, Vol. 38 ›› Issue (1): 217-222.doi: 10.1007/s40242-021-1358-1

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Remote Synthesis of Layered Double Hydroxide Nanosheets Through the Automatic Chemical Robot

WANG Zelin¹, LIU Guihao², SHEN Tianyang², TAN Ling², ZHAO Yufei², SONG Yu-Fei^2,3

1. CNPC Research Institute of Safety and Environmental Technology, Beijing 102206, P. R. China;
2. State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, P. R. China;
3. Beijing Advanced Innovation Center for Soft Matter Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, P. R. China

Received:2021-09-06 Revised:2021-09-26 Online:2022-02-01 Published:2021-10-08
Contact: SONG Yu-Fei, ZHAO Yufei E-mail:songyf@mail.buct.edu.cn；zhaoyufei@mail.buct.edu.cn
Supported by:
This work was supported by the National Natural Science Foundation of China (Nos.21922801, 21878008) and the Beijing Natural Science Foundation, China (Nos.2202036, 2182047). The XAFS experiments were conducted in 1W1B beamline of the Beijing Synchrotron Radiation Facility(BSRF), China.

Abstract

Abstract: As a family of two-dimensional functional materials, layered double hydroxides(LDHs) have the characteristics of adjustable lamellar element type and proportion, variable interlamellar anion, controllable particle size and thickness, providing a robust platform for photo/electro/thermal-catalysis. With the continuous progress of materials science, the synthesis of LDHs is becoming more and more refined. Herein, to achieve the fine preparation of LDHs materials, especailly for the no-chemical/material researchers, we successfully assembled the automatic synthesis device and wrote corresponding computer software to control this device, and the automatic synthesis of bulk and monolayer LDHs nanosheets on a laboratory scale can be realized. This work paves a new labor-saving way for the fine synthesis of LDHs nanostructures, further improving the development of LDHs-based materials.

Key words: Layered double hydroxide, Automatic synthesis, Monolayer, Single-atom catalyst

WANG Zelin, LIU Guihao, SHEN Tianyang, TAN Ling, ZHAO Yufei, SONG Yu-Fei. Remote Synthesis of Layered Double Hydroxide Nanosheets Through the Automatic Chemical Robot[J]. Chemical Research in Chinese Universities, 2022, 38(1): 217-222.

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Remote Synthesis of Layered Double Hydroxide Nanosheets Through the Automatic Chemical Robot

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