HEDP-capped Terbium Orthophosphate Nanoparticles as Sensitive Luminescent Probes for the Detection of Pb2+ Ions

doi:10.1007/s40242-016-6005-x

Abstract

Abstract:

Terbium orthophosphate nanoparticles were synthesized using 1-hydroxy ethylidene-1,1-diphosphonic acid(HEDP) as a capping ligand under hydrothermal conditions at 80℃. These HEDP-capped TbPO₄ nanoparticles owned a hexagonal phase structure according to the powder X-ray diffraction(XRD) results and were spherical monodispersed particles with a diameter of about 10 nm confirmed by transimission electron microscope(TEM) images. Interestingly, the luminescent intensities of the HEDP-capped TbPO₄ nanoparticles decreased obviously in the presence of Pb²⁺ ions and such a quenching behavior of luminescence was well fitted by the Stern-Volmer equation.

Key words: Lanthanide nanoparticle, Hydrothermal synthesis, Detection of Pb²⁺, Luminescent probe

WANG Xi, HAN Bin, GAO Yan, WANG Li, BAI Ming. HEDP-capped Terbium Orthophosphate Nanoparticles as Sensitive Luminescent Probes for the Detection of Pb²⁺ Ions[J]. Chemical Research in Chinese Universities, 2016, 32(3): 325-328.

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HEDP-capped Terbium Orthophosphate Nanoparticles as Sensitive Luminescent Probes for the Detection of Pb²⁺ Ions

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