Synthesis of NiFe2O4 Nanowires with NiO Nanosheet as Precursor via a Topochemical Solid State Method

doi:10.1007/s40242-015-5132-0

Chemical Research in Chinese Universities ›› 2015, Vol. 31 ›› Issue (5): 885-889.doi: 10.1007/s40242-015-5132-0

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Synthesis of NiFe₂O₄ Nanowires with NiO Nanosheet as Precursor via a Topochemical Solid State Method

FENG Jing¹, HOU Xiangyu², CHEN Tingting¹, LIU Shengna¹, FAN Zhuangjun¹, REN Yueming¹, LÜ Yanzhuo¹

1. Key Laboratory of Superlight Materials & Surface Technology, Ministry of Education, Harbin Engineering University, Harbin 150001, P. R. China;
2. Institute of Seawater Desalination and Multipurpose Utilization, State Oceanic Administration, Tianjin 300192, P. R. China

Received:2015-04-03 Revised:2015-07-15 Online:2015-10-01 Published:2015-10-10
Contact: FENG Jing, E-mail: fengjing@hrbeu.edu.cn; FAN Zhuangjun, E-mail: fanzhj666@163.com E-mail:fengjing@hrbeu.edu.cn;fanzhj666@163.com
Supported by:
Supported by the National Natural Science Foundation of China(Nos.21301038, 51108111, 21203040), the Fundamental Research Funds for the Central Universities of China(No.HEUCF2015003) and the Natural Science Foundation of Heilongjiang Province of China(No.B201201).

Abstract

Abstract:

Large scale NiFe₂O₄ nanowires were synthesized with NiO nanosheets as precursor by means of the topochemical solid state method. The morphologies and magnetic properties of NiFe₂O₄ annealed at different temperatures were studied. An appropriate annealing temperature was requested to transfer NiO nanosheets and Fe^- ions into NiFe₂O₄ nanowires. In the beginning stage of synthesizing process, the shape of NiO nanosheets remained unchanged at low temperatures. And then, NiO nanosheets split into nanowires from 400℃ to 600℃. At last they transformed into nanoparticles from 700℃ to 1000℃. Thus, the optimized annealing temperature was selected as 600℃ because the NiFe₂O₄ obtained at 600℃(N600) exhibited a maximum aspect ratio of 50 with a diameter of 20 nm and a length of 1 μm. Furthermore, N600 also displayed the largest magnetization value of 26.86 A·m²/kg and the lowest coercivity(H_c) of 8914 A/m.

Key words: Nanowire, NiO, NiFe₂O₄, Solid state method, Topochemical method

FENG Jing, HOU Xiangyu, CHEN Tingting, LIU Shengna, FAN Zhuangjun, REN Yueming, LÜ Yanzhuo. Synthesis of NiFe₂O₄ Nanowires with NiO Nanosheet as Precursor via a Topochemical Solid State Method[J]. Chemical Research in Chinese Universities, 2015, 31(5): 885-889.

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Synthesis of NiFe₂O₄ Nanowires with NiO Nanosheet as Precursor via a Topochemical Solid State Method

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