Fabrication, Characterization and Optical Properties of TiO2 Nanotube Arrays on Boron-doped Diamond Film Through Liquid Phase Deposition

doi:10.1007/s40242-014-3320-y

Chemical Research in Chinese Universities ›› 2014, Vol. 30 ›› Issue (1): 18-22.doi: 10.1007/s40242-014-3320-y

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Fabrication, Characterization and Optical Properties of TiO₂ Nanotube Arrays on Boron-doped Diamond Film Through Liquid Phase Deposition

YUAN Jüjun^1,2,3, LI Hongdong², WANG Qiliang², CHENG Shaoheng², ZHANG Xianke¹, YU Huajun¹, ZHU Xiurong¹, XIE Yingmao¹

1. College of Physics and Electronics, Gannan Normal University, Ganzhou 341000, P. R. China;
2. State Key Laboratory of Superhard Materials, Jilin University, Changchun 130012, P. R. China;
3. Institute of Optoelectronic Materials and Technology, Gannan Normal University, Ganzhou 341000, P. R. China

Received:2013-07-29 Revised:2013-10-10 Online:2014-02-01 Published:2013-10-23
Contact: LI Hongdong,E-mail:hdli@jlu.edu.cn E-mail:hdli@jlu.edu.cn
Supported by:
Supported by the National Natural Science Foundation of China(Nos.51072066, 11247305), the PhD Programs Foundation of Ministry of Education of China(No.20100061110083), the Open Project of State Key Laboratory of Superhard Materials(Jilin University), China(No.201213) and the Youth Fund of Science and Technology Department of Jiangxi Province, China (No.20131522040044).

Abstract

Abstract:

TiO₂ nanotube(TiNT) arrays were deposited on boron-doped diamond films by a liquid-phase deposition method with ZnO nanorod arrays as the template. The different morphologies of TiNTs have been obtained by controlling the morphology of ZnO template. The X-ray diffraction and energy-dispersive X-ray analysis show that the ZnO nanorod array template has been removed in the TiNTs formation process. The crystalline quality of the TiNTs is improved by increasing the annealing temperature. The band gap of the TiNTs is about 3.25 eV estimated by the UV-Vis absorption spectroscopy, which is close to the value of bulk TiO₂. In the photoluminescence spectrum, a broad visible emission in a range of ca. 550—750 nm appears due to the surface oxygen vacancies and defects.

Key words: TiO₂ nanotube array, Boron doped diamond, Lquid phase deposition, Optical property

YUAN Jüjun, LI Hongdong, WANG Qiliang, CHENG Shaoheng, ZHANG Xianke, YU Huajun, ZHU Xiurong, XIE Yingmao. Fabrication, Characterization and Optical Properties of TiO₂ Nanotube Arrays on Boron-doped Diamond Film Through Liquid Phase Deposition[J]. Chemical Research in Chinese Universities, 2014, 30(1): 18-22.

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Fabrication, Characterization and Optical Properties of TiO₂ Nanotube Arrays on Boron-doped Diamond Film Through Liquid Phase Deposition

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