Synthesis and Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)2][NiQ3](ClO4)

Chemical Research in Chinese Universities ›› 1990, Vol. 6 ›› Issue (4): 271-275.

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Synthesis and Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)₂][NiQ₃](ClO₄)

Zhang Mingjie, Huang Chunhui, Xu Guangxian

Chemistry Department, Peking University, Beijing

Received:1990-06-17 Online:1990-12-24 Published:2011-09-09

Abstract

Abstract: The title compound was synthesised and the X-ray diffraction analysis shows that the crystal belongs to in monoclinic system, space group P2₁/n with α=16.972(4) A ,b=14.128(3)A , c=22.615(4)A ,β=103.16(2)°,V=528.14A³,F(000)=2264, Z=4. Both cation [YQ(HQ)₂]²⁺ and anion [NiQ₃]^- are of distorded octahedral geometry with coordination number of 6. Its IRspectrum was recorded.

Key words: 8-Quinolinol, Yttrium, Nickel, Complex, Crystal structure

Zhang Mingjie, Huang Chunhui, Xu Guangxian . Synthesis and Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)₂][NiQ₃](ClO₄)[J]. Chemical Research in Chinese Universities, 1990, 6(4): 271-275.

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Synthesis and Crystal Structure of Tri(8-quinolinol) Yttrium-Tri(8-quinolinol) Nickel Perchlorate [YQ(HQ)₂][NiQ₃](ClO₄)

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