Deposition of Phosphate Nanoparticles onto Textile Fabrics via Sol-gel Method and Their Kinetics Desorption Studies

doi:10.1007/s40242-020-0045-y

Chemical Research in Chinese Universities ›› 2020, Vol. 36 ›› Issue (5): 877-884.doi: 10.1007/s40242-020-0045-y

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Deposition of Phosphate Nanoparticles onto Textile Fabrics via Sol-gel Method and Their Kinetics Desorption Studies

Mohamed El MESSOUDI^1,2,3, Aicha BOUKHRISS¹, Laila SADALLAH², Laila SAJID^4,5, M'hamed El KOUALI³, Said GMOUH²

1. Laboratory REMTEX, ESITH, Higher School of Textile and Clothing Industries(ESITH), Km8, Route d'EL JADIDA, Casablanca, Morocco;
2. Laboratory LIMAT, Faculty of Sciences Ben M'Sik, Hassan II University of Casablanca, B. P 5366 Maarif, Casablanca, Morocco;
3. Laboratory LCAPCM, Faculty of Sciences Ben M'Sik, Hassan II University of Casablanca, B. P 5366 Maarif, Casablanca, Morocco;
4. Laboratory L3 GIE, Mohammadia School of Engineers, Mohammad V University, BP. 765 Av. Ibn Sina, Agdal, Rabat, Morocco;
5. Laboratory LEC, Higher School of Textile and Clothing Industries(ESITH), Km 8, Route d'EL JADIDA, Casablanca, Morocco

Received:2020-02-27 Revised:2020-06-05 Online:2020-10-01 Published:2020-10-01
Contact: Said GMOUH E-mail:s.gmouh1@gmail.com
Supported by:
Supported by the National Center for Scientific and Technical Research(CNRST) under the Program Research Excellence Scholarships, Morocco.

Abstract

Abstract: In this paper, phosphate nanoparticles were coated on cotton(CO) and polyester(PES) textile surfaces by sol-gel method using tetraethylorthosilicate(TEOS) and chloropropyltriethoxysilane(CPTS) as silica precursors. The deposited nanoparticles were observed with scanning electronic microscopy energy-dispersive X-ray spectroscopy (SEM-EDX). The release kinetics of phosphorus(P) from these textiles into the aqueous medium(Aq), acid(Ac), and basic(Ba) artificial sweats were then studied. The released amount of phosphorus was evaluated by the inductively coupled plasma(ICP) according to ISO NF EN 16711-2 procedure. The results revealed that the release of P into the aqueous medium is lower than in the artificial sweat. The kinetics data[the phosphorus desorption amount(mg/g) as a function of time] were modeled according to five models:the first order, the second order, the third order, simple Elovich and parabolic diffusion. The suitable model was chosen based on the coefficient of determination(R²) and the calculation of the sum of the absolute errors(EABS), which describes the error between the theoretical and experimental values. SEM observations were also carried out on the fabrics after desorption in order to show the impact of desorption on their morphology. Furthermore, the impact of P release on the tensile strength of CO and PES fabrics was investigated using a uniaxial tensile test. The thermal stability of all samples before and after desorption was assessed by thermogravimetric analysis(ATG).

Key words: Sol-gel, Coating, Kinetic, Desorption, Phosphate nanoparticle

Mohamed El MESSOUDI, Aicha BOUKHRISS, Laila SADALLAH, Laila SAJID, M'hamed El KOUALI, Said GMOUH. Deposition of Phosphate Nanoparticles onto Textile Fabrics via Sol-gel Method and Their Kinetics Desorption Studies[J]. Chemical Research in Chinese Universities, 2020, 36(5): 877-884.

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Deposition of Phosphate Nanoparticles onto Textile Fabrics via Sol-gel Method and Their Kinetics Desorption Studies

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