Electrospinning Preparation of β-Cyclodextrin/Glutaraldehyde Crosslinked PVP Nanofibrous Membranes to Adsorb Dye in Aqueous Solution

doi:10.1007/s40242-014-4203-y

Abstract

Abstract:

The insoluble β-cyclodextrin/glutaraldehyde crosslinked polyvinylpyrrolidone nanofibrous membranes were prepared by electrospinning technique. The membranes were extensively characterized by various techniques including attenuated total reflectance Fourier transform infrared spectroscopy(ATR-FTIR), X-ray diffraction(XRD), scanning electron microscopy(SEM) and UV-visible absorption to correlate membrane characteristics with their performance. The adsorption ability of the nanofibrous membranes was tested by performing extraction of Methyl orange(MO) dye in water. It was observed that β-cyclodextrin incorporated in polyvinylpyrrolidone provided the characteristics of high adsorption capacity of polyvinylpyrrolidone. Results of sorption experiments show that the nanofibrous membranes exhibited an adsorption rate of more than 95% for MO and the MO absorbent was 39.82 mg to per gram of β-cyclodextrin glutaraldehyde(β-CDXFM) crosslinked PVP under the optimized experimental conditions.

Key words: β-Cyclodextrin, Glutaraldehyde, Polyvinylpyrrolidone, Adsorption, Nanofibrous membrane

XIAO Ning, WEN Qian, LIU Qingwen, YANG Qingbiao, LI Yaoxian. Electrospinning Preparation of β-Cyclodextrin/Glutaraldehyde Crosslinked PVP Nanofibrous Membranes to Adsorb Dye in Aqueous Solution[J]. Chemical Research in Chinese Universities, 2014, 30(6): 1057-1062.

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