Hydrothermal Syntheses, Crystal Structures and Thermal Properties of Two New Organically Templated Open-framework Gallium Phosphites

doi:10.1007/s40242-013-2212-x

高等学校化学研究 ›› 2013, Vol. 29 ›› Issue (2): 201-205.doi: 10.1007/s40242-013-2212-x

Hydrothermal Syntheses, Crystal Structures and Thermal Properties of Two New Organically Templated Open-framework Gallium Phosphites

ZHOU Guang-peng^1,2, YANG Yu-lin¹, FAN Rui-qing¹, XIE Jia-qing², QUAN Xue-jun²

1. Department of Chemistry, Harbin Institute of Technology, Harbin 150001, P. R. China;
2. College of Chemistry and Chemical Engineering, Chongqing University of Technology, Chongqing 400050, P. R. China

收稿日期:2012-05-31 修回日期:2012-09-06 出版日期:2013-04-01 发布日期:2013-03-20
通讯作者: YANG Yu-lin, FAN Rui-qing E-mail:ylyang@hit.edu.cn;fanruiqing@163.com
基金资助:
Supported by the National Natural Science Foundation of China(Nos.20971031, 21071035, 21171044), the National Key Basic Research Program of China(No.2013CB632900) and the Key Natural Science Foundation of Heilongjiang Province of China (No.ZD201009).

Hydrothermal Syntheses, Crystal Structures and Thermal Properties of Two New Organically Templated Open-framework Gallium Phosphites

ZHOU Guang-peng^1,2, YANG Yu-lin¹, FAN Rui-qing¹, XIE Jia-qing², QUAN Xue-jun²

1. Department of Chemistry, Harbin Institute of Technology, Harbin 150001, P. R. China;
2. College of Chemistry and Chemical Engineering, Chongqing University of Technology, Chongqing 400050, P. R. China

Received:2012-05-31 Revised:2012-09-06 Online:2013-04-01 Published:2013-03-20
Supported by:
Supported by the National Natural Science Foundation of China(Nos.20971031, 21071035, 21171044), the National Key Basic Research Program of China(No.2013CB632900) and the Key Natural Science Foundation of Heilongjiang Province of China (No.ZD201009).

摘要/Abstract

摘要：

Two new open-framework gallium phosphites formulated as (C₂N₂H₁₀)_0.5Ga₂(OH)(H₂O)(HPO₃)₃(1) and (C₃N₂H₅)₂(C₃N₂H₆)Ga₈(H₂O)₆(HPO₃)₁₄(2) were hydrothermally synthesized in the presence of ethylenediamine(en) and imidazole as structure directing agents(SDA), respectively. Structural analyses reveal that the 3D structures of compounds 1 and 2 are both built up from the linkage of GaO₆, GaO₅(H₂O) and HPO₃^2? units by sharing vertices. The structure of compound 2 is constructed from well-known 4.6.12-net connecting layers in the AAAA stacking sequence, which are penetrated by the 1D Ga-O-P chains to form a 3D pillared-layered structure.

关键词: Hydrothermal synthesis, Crystal structure, Gallium phosphite

Abstract:

Key words: Hydrothermal synthesis, Crystal structure, Gallium phosphite

ZHOU Guang-peng, YANG Yu-lin, FAN Rui-qing, XIE Jia-qing, QUAN Xue-jun. Hydrothermal Syntheses, Crystal Structures and Thermal Properties of Two New Organically Templated Open-framework Gallium Phosphites[J]. 高等学校化学研究, 2013, 29(2): 201-205.

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Hydrothermal Syntheses, Crystal Structures and Thermal Properties of Two New Organically Templated Open-framework Gallium Phosphites

Hydrothermal Syntheses, Crystal Structures and Thermal Properties of Two New Organically Templated Open-framework Gallium Phosphites

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