Chemical Research in Chinese Universities ›› 2014, Vol. 30 ›› Issue (3): 405-408.doi: 10.1007/s40242-014-3417-3

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Mild and Efficient Synthesis of 1-(6-Chloroquinoxalin-2-yl)-2-[4-(trifluoromethyl)-2,6-dinitrophenyl] Hydrazine Derivatives by Microwave Irradiation

MILAD Taheri, HANIYEH Alavi, HAMIDEH Nazari   

  1. Department of Chemistry, Islamic Azad University, Tehran 14735/334, Iran
  • Received:2013-09-30 Revised:2013-12-09 Online:2014-06-01 Published:2014-05-24
  • Contact: MILAD Taheri E-mail:miladtaheri1@hotmail.co.uk

Abstract:

Some 1-(6-chloroquinoxalin-2-yl)-2-[4-(trifluoromethyl)-2,6-dinitrophenyl] hydrazine derivatives have been synthesized via both conventional and microwave assisted organic synthesis(MAOS) methods. The MAOS method is more effective on synthesizing these compounds than the conventional method in regard to the higher chemical yields of products(76%―98%) and the shorter reaction time(1―15 min).

Key words: 2,6-Dichloroquinoxaline, 2-Chloro-1-3-dinitro-5-triflouromthylbenzene hydrazine hydrate, Methyl hydrazine, Microwave assistant organic synthesis(MAOS)