One-pot Three-component Synthesis of 4,4′-Arylidene-bis(3-methyl-pyrazolones) Derivatives in Water

高等学校化学研究 ›› 2012, Vol. 28 ›› Issue (6): 999-1002.

One-pot Three-component Synthesis of 4,4′-Arylidene-bis(3-methyl-pyrazolones) Derivatives in Water

JIA Xu-dong, DUAN Hai-feng, LIN Ying-jie, CAO Jun-gang, LIANG Da-peng, WU Mao-cheng

Department of Organic Chemistry, College of Chemistry, Jilin University, Changchun 130012, P. R. China

收稿日期:2011-12-05 修回日期:2012-01-13 出版日期:2012-11-25 发布日期:2012-11-09
通讯作者: DUAN Hai-feng, LIN Ying-jie E-mail:duanhf@jlu.edu.cn;linyj@jlu.edu.cn

One-pot Three-component Synthesis of 4,4′-Arylidene-bis(3-methyl-pyrazolones) Derivatives in Water

JIA Xu-dong, DUAN Hai-feng, LIN Ying-jie, CAO Jun-gang, LIANG Da-peng, WU Mao-cheng

Department of Organic Chemistry, College of Chemistry, Jilin University, Changchun 130012, P. R. China

Received:2011-12-05 Revised:2012-01-13 Online:2012-11-25 Published:2012-11-09
Contact: DUAN Hai-feng, LIN Ying-jie E-mail:duanhf@jlu.edu.cn;linyj@jlu.edu.cn

摘要/Abstract

摘要：

Aldehydes, hydrazine and ethyl acetoacetate were used for the synthesis of 4,4′-arylidene-bis (3-methyl-pyrazolones) derivatives in water. In this green synthetic protocol, the solvent water itself catalyzed the reaction via hydrogen bonding, thus avoiding the use of any other catalyst to make the work up procedure easier. One-pot, environmental friendly and convenient are the highlights.

关键词: 4,4′-Arylidene-bis(3-methyl-pyrazolones), Catalysis, Multi-component reaction

Abstract:

Key words: 4,4′-Arylidene-bis(3-methyl-pyrazolones), Catalysis, Multi-component reaction

JIA Xu-dong, DUAN Hai-feng, LIN Ying-jie, CAO Jun-gang, LIANG Da-peng, WU Mao-cheng . One-pot Three-component Synthesis of 4,4′-Arylidene-bis(3-methyl-pyrazolones) Derivatives in Water[J]. 高等学校化学研究, 2012, 28(6): 999-1002.

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One-pot Three-component Synthesis of 4,4′-Arylidene-bis(3-methyl-pyrazolones) Derivatives in Water

One-pot Three-component Synthesis of 4,4′-Arylidene-bis(3-methyl-pyrazolones) Derivatives in Water

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