Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique

高等学校化学研究 ›› 2010, Vol. 26 ›› Issue (5): 675-677.

Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique

HU Shi-qi, HUANG Ke-ke, HOU Chang-min, YUAN Hong-ming, HU Bin and FENG Shou-hua*

State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, P. R. China

收稿日期:2009-09-24 修回日期:2009-11-15 出版日期:2010-09-25 发布日期:2010-11-26
通讯作者: FENG Shou-hua. E-mail: shfeng@jlu.edu.cn
基金资助:
Supported by the National Natural Science Foundation of China(Nos.20631010 and 90922034) and the Graduate Innovation Fund of “985” Program of Jilin University, China.

Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique

HU Shi-qi, HUANG Ke-ke, HOU Chang-min, YUAN Hong-ming, HU Bin and FENG Shou-hua*

State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, P. R. China

Received:2009-09-24 Revised:2009-11-15 Online:2010-09-25 Published:2010-11-26
Contact: FENG Shou-hua. E-mail: shfeng@jlu.edu.cn
Supported by:
Supported by the National Natural Science Foundation of China(Nos.20631010 and 90922034) and the Graduate Innovation Fund of “985” Program of Jilin University, China.

摘要/Abstract

摘要： ZnO particles were prepared by Au-catalyzed vapor phase transport method on silicon substrate. Scanning electron microscopy(SEM) images show many ZnO particles were formed on the sample surface. They grew up layer by layer along the c-axis, which was confirmed by the results of X-ray diffraction(XRD). The morphology of ZnO particles is close to hemisphere and its formation process could be seen from the SEM image. The room temperature photoluminescence(PL) measurement revealed a narrow UV emission peak at 3.27 eV and a broad green emission peak at 2.45 eV, which was caused by the near-band-edge and deep-level emissions.

关键词: ZnO, Au-catalyzed, Vapor phase transport, Photoluminescence

Abstract: ZnO particles were prepared by Au-catalyzed vapor phase transport method on silicon substrate. Scanning electron microscopy(SEM) images show many ZnO particles were formed on the sample surface. They grew up layer by layer along the c-axis, which was confirmed by the results of X-ray diffraction(XRD). The morphology of ZnO particles is close to hemisphere and its formation process could be seen from the SEM image. The room temperature photoluminescence(PL) measurement revealed a narrow UV emission peak at 3.27 eV and a broad green emission peak at 2.45 eV, which was caused by the near-band-edge and deep-level emissions.

Key words: ZnO, Au-catalyzed, Vapor phase transport, Photoluminescence

HU Shi-qi, HUANG Ke-ke, HOU Chang-min, YUAN Hong-ming, HU Bin and FENG Shou-hua*. Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique[J]. 高等学校化学研究, 2010, 26(5): 675-677.

HU Shi-qi, HUANG Ke-ke, HOU Chang-min, YUAN Hong-ming, HU Bin and FENG Shou-hua*. Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique[J]. Chemical Research in Chinese Universities, 2010, 26(5): 675-677.

参考文献

[1] Ye H. Y., Lai H. W., Wu S. J., Cui X. H., Kan Q. B., Chem. J. Chinese Universities, 2007, 28(2), 312 [2] Zhang X. R., Gu X. W., Sun J., Xu Z., Chem. J. Chinese Universities, 2006, 27(8), 1555 [3] Xing Y. J., Xi Z. H., Xue Z. Q., Zhang X. D., Song J. H., Wang R. M., Xu J., Song Y., Zhang S. L., Yu D. P., Appl. Phys. Lett., 2003, 83, 1689 [4] Lee J. S., Park K., Kang M., Park I. W., Kim S. W., Cho W. K., Han H. S., Kim S., J. Crystal Growth, 2003, 254, 423 [5] Xu X. C., Sun X. W., Chen B. J., Shun P., Li S., Hu X., J. Appl. Phys., 2004, 95, 661 [6] Pan Z. W., Dai Z. R., Wang Z. L., Science, 2001, 291, 1947 [7] Kong X. Y., Wang Z. L., Nano Lett., 2003, 3, 1625 [8] Kong X. Y., Ding Y., Yang R. S., Wang Z. L., Science, 2004, 303, 1348 [9] Yang P. D., Yan H. Q., Mao S., Russo R., Johnson J., Saykally R., Morris N., Pham J., He R. R., Choi H. J., Adv. Funct. Mater., 2002, 12, 323 [10] Bai Z. G., Yu D. P., Zhang H. Z., Ding Y., Gai X. Z., Hang Q. L., Xiong G. C., Feng S. Q., Chem. Phys. Lett., 1999, 303, 311 [11] Park W. I., Kim D. H., Jung S. W., Yi G. C., Appl. Phys. Lett., 2002, 80, 4232 [12] Vayssieres L., Keis K., Lindquist S. E., Hagfeldt A., J. Phys. Chem. B, 2001, 105, 3350 [13] Zhang M. J., Zhang L. D., Li G. H., Shen W. Z., Chem. Phys. Lett., 2002, 363, 123 [14] Bethke S., Pan H., Wessels B. W., Appl. Phys. Lett., 1988, 52, 138 [15] Yang L. W., Wu X. L., Xiong Y., Yang Y. M., Huang G. S., Chu P. K., Siu G. G., Journal of Crystal Growth, 2005, 283, 332 [16] Yeadon M., Ghaly M., Yang J. C., Averback R. S., Gibson J. M., Appl. Phys. Lett., 1998, 73, 3208 [17] Kong Y. C., Yu D. P., Zhang B., Fang W., Feng S. Q., Appl. Phys. Lett., 2001, 78, 407 [18] Vanheusden K., Warren W. L., Seager C. H., Tallant D. K., Voigt J. A., Gnade B. E., J. Appl. Phys., 1996, 79, 7983

Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique

Characteristics of ZnO Particles Prepared by Au-catalyzed Phase Transport Technique

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