高等学校化学研究 ›› 2010, Vol. 26 ›› Issue (3): 344-347.
LI Hai-bo1*, XU Shi-chong1,2, LIU Mei1, FENG Ming1,2 and YIN Ji-zhe1
LI Hai-bo1*, XU Shi-chong1,2, LIU Mei1, FENG Ming1,2 and YIN Ji-zhe1
摘要: The soft magnetic nanocomposites with equiatomic FeCo particles dispersed in Al2O3 matrix were synthesized via a sol-gel technique combined with H2 reduction method. The samples were characterized by X-ray diffraction, transmission electron microscopy and vibrating sample magnetometer. The FeCo nanoparticles in all the samples have the typical bcc structure. With the decreasing of Al2O3 content, the mean grain size of FeCo in the nanocomposites and the saturation magnetization of the samples increase, while the coercivity of samples increases firstly and then decreases due to different magnetic mechanisms.