Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids

高等学校化学研究 ›› 2004, Vol. 20 ›› Issue (2): 213-215.

Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids

LIN Min¹, ZHOU Jin-mei¹, XIA Hai-ping², YANG Rui-feng¹, LIN Chen¹

1. Department of Chemistry, Xiamen 361005, P.R. China;
2. Department of Material Sciences, Xiamen University, Xiamen 361005, P.R. China

收稿日期:2003-12-05 出版日期:2004-04-24 发布日期:2011-08-06

Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids

LIN Min¹, ZHOU Jin-mei¹, XIA Hai-ping², YANG Rui-feng¹, LIN Chen¹

1. Department of Chemistry, Xiamen 361005, P.R. China;
2. Department of Material Sciences, Xiamen University, Xiamen 361005, P.R. China

Received:2003-12-05 Online:2004-04-24 Published:2011-08-06

摘要/Abstract

摘要： Several aryloxy acetic acids were synthesized under microwave irradiation. The factors, which affect the reaction, were investigated and optimized. It was revealed that the best yields(92.7%-97.4%) were obtained when the molar ratio of the reactants was n(ArOH) : n(NaOH): n(ClCH₂CO₂H) =1: 2.5: 1.2 with microwave irradiation power of 640 W for 65-85 s.

关键词: Microwave irradiation, Aryloxy acetic acid, Synthesis

Abstract: Several aryloxy acetic acids were synthesized under microwave irradiation. The factors, which affect the reaction, were investigated and optimized. It was revealed that the best yields(92.7%-97.4%) were obtained when the molar ratio of the reactants was n(ArOH) : n(NaOH): n(ClCH₂CO₂H) =1: 2.5: 1.2 with microwave irradiation power of 640 W for 65-85 s.

Key words: Microwave irradiation, Aryloxy acetic acid, Synthesis

LIN Min, ZHOU Jin-mei, XIA Hai-ping, YANG Rui-feng, LIN Chen. Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids[J]. 高等学校化学研究, 2004, 20(2): 213-215.

LIN Min, ZHOU Jin-mei, XIA Hai-ping, YANG Rui-feng, LIN Chen. Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids[J]. Chemical Research in Chinese Universities, 2004, 20(2): 213-215.

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Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids

Microwave Irradiation Promoted Synthesis of Aryloxy Acetic Acids

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