CO2/NOx-involved Electrochemical C-N Coupling Reactions

doi:10.1007/s40242-024-4118-1

高等学校化学研究 ›› 2024, Vol. 40 ›› Issue (5): 764-775.doi: 10.1007/s40242-024-4118-1

CO₂/NO_x-involved Electrochemical C-N Coupling Reactions

SUI Xiqing^1,2, WU Limin^1,2, JIA Shunhan^1,2, JIN Xiangyuan^1,2, SUN Xiaofu^1,2, HAN Buxing^1,2,3

1. Beijing National Laboratory for Molecular Sciences, Key Laboratory of Colloid and Interface and Thermodynamics, Center for Carbon Neutral Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, P. R. China;
2. School of Chemical Sciences, University of Chinese Academy of Sciences, Beijing 100049, P. R. China;
3. Shanghai Key Laboratory of Green Chemistry and Chemical Processes, School of Chemistry and Molecular Engineering, East China Normal University, Shanghai 200062, P. R. China

收稿日期:2024-05-08 出版日期:2024-10-01 发布日期:2024-09-26
通讯作者: SUN Xiaofu,sunxiaofu@iccas.ac.cn;HAN Buxing,hanbx@iccas.ac.cn E-mail:sunxiaofu@iccas.ac.cn;hanbx@iccas.ac.cn
基金资助:
This work was supported by the National Natural Science Foundation of China (Nos.22293015,22121002),the Beijing Natural Science Foundation,China (No.J210020),the Strategic Priority Research Program (A) of the Chinese Academy of Sciences (No.XDA0390400),and the Project of the Photon Science Center for Carbon Neutrality of CAS.

CO₂/NO_x-involved Electrochemical C-N Coupling Reactions

SUI Xiqing^1,2, WU Limin^1,2, JIA Shunhan^1,2, JIN Xiangyuan^1,2, SUN Xiaofu^1,2, HAN Buxing^1,2,3

1. Beijing National Laboratory for Molecular Sciences, Key Laboratory of Colloid and Interface and Thermodynamics, Center for Carbon Neutral Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, P. R. China;
2. School of Chemical Sciences, University of Chinese Academy of Sciences, Beijing 100049, P. R. China;
3. Shanghai Key Laboratory of Green Chemistry and Chemical Processes, School of Chemistry and Molecular Engineering, East China Normal University, Shanghai 200062, P. R. China

Received:2024-05-08 Online:2024-10-01 Published:2024-09-26
Contact: SUN Xiaofu,sunxiaofu@iccas.ac.cn;HAN Buxing,hanbx@iccas.ac.cn E-mail:sunxiaofu@iccas.ac.cn;hanbx@iccas.ac.cn
Supported by:
This work was supported by the National Natural Science Foundation of China (Nos.22293015,22121002),the Beijing Natural Science Foundation,China (No.J210020),the Strategic Priority Research Program (A) of the Chinese Academy of Sciences (No.XDA0390400),and the Project of the Photon Science Center for Carbon Neutrality of CAS.

摘要/Abstract

摘要： With the excessive use of fossil fuels leading to significant CO₂ emissions, and the continuous increase of NO_x in water bodies and soils, the use of electrochemical methods for the conversion of CO₂ and NO_x has garnered widespread attention as a green chemical approach due to its advantages of being environmentally friendly, low-carbon, and straightforward. C—N bonds are widely present in many value-added chemicals, such as urea, amides, and oximes. However, traditional methods for constructing C—N bonds typically involve thermochemical processes. Therefore, using electrochemical methods to catalyze the reduction of CO₂ and NO_x for C—N bond formation has emerged as a green and sustainable alternative. This paper summarizes the research progress of electrochemical C—N bond construction involving CO₂ and NO_x from the perspectives of reaction mechanisms and catalytic system construction, reviews the electrochemical synthesis of urea, amines, amides, and oximes through electrochemical C—N bond construction, and finally analyzes the current problems and challenges in the field, providing prospects for its future development.

关键词: CO₂ reduction, NO_x reduction, C-N coupling, Electro-catalysis

Abstract: With the excessive use of fossil fuels leading to significant CO₂ emissions, and the continuous increase of NO_x in water bodies and soils, the use of electrochemical methods for the conversion of CO₂ and NO_x has garnered widespread attention as a green chemical approach due to its advantages of being environmentally friendly, low-carbon, and straightforward. C—N bonds are widely present in many value-added chemicals, such as urea, amides, and oximes. However, traditional methods for constructing C—N bonds typically involve thermochemical processes. Therefore, using electrochemical methods to catalyze the reduction of CO₂ and NO_x for C—N bond formation has emerged as a green and sustainable alternative. This paper summarizes the research progress of electrochemical C—N bond construction involving CO₂ and NO_x from the perspectives of reaction mechanisms and catalytic system construction, reviews the electrochemical synthesis of urea, amines, amides, and oximes through electrochemical C—N bond construction, and finally analyzes the current problems and challenges in the field, providing prospects for its future development.

Key words: CO₂ reduction, NO_x reduction, C-N coupling, Electro-catalysis

SUI Xiqing, WU Limin, JIA Shunhan, JIN Xiangyuan, SUN Xiaofu, HAN Buxing. CO₂/NO_x-involved Electrochemical C-N Coupling Reactions[J]. 高等学校化学研究, 2024, 40(5): 764-775.

SUI Xiqing, WU Limin, JIA Shunhan, JIN Xiangyuan, SUN Xiaofu, HAN Buxing. CO₂/NO_x-involved Electrochemical C-N Coupling Reactions[J]. Chemical Research in Chinese Universities, 2024, 40(5): 764-775.

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CO₂/NO_x-involved Electrochemical C-N Coupling Reactions

CO₂/NO_x-involved Electrochemical C-N Coupling Reactions

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