高等学校化学研究 ›› 1999, Vol. 15 ›› Issue (2): 105-109.
Preparation of LiTi2(PO4)3 by the Solgel Method, Investigation of Its Formation Process
ZHU Ji-shun1, Tohge Noboru2, Minami Tsutomu2
- 1. Department of Chemistry, Shanghai Normal University, Shanghai, 200234;
2. Department of Applied Chemistry, University of Osaka Prefecture, 4-804, Mozu-umemachi, Sakai-shi, Osaka 591, Japan
Preparation of LiTi2(PO4)3 by the Solgel Method, Investigation of Its Formation Process
ZHU Ji-shun1, Tohge Noboru2, Minami Tsutomu2
- 1. Department of Chemistry, Shanghai Normal University, Shanghai, 200234;
2. Department of Applied Chemistry, University of Osaka Prefecture, 4-804, Mozu-umemachi, Sakai-shi, Osaka 591, Japan
摘要： In this study, a novel sol-gel method has been developed to prepare LiTi2(PO4)3 lithium ion conductor as monophase at relatively low temperature(600℃). According to the XRD, IR analysis, the as-prepared sample remained an amorphous state up to 500℃. The activation energy was calculated to be 252 kJ/mol according to the modified Kissinger equation.