Detection of Amines in Lamb Spoilage by Optical Waveguide Sensor Based on Bromophenol Blue-Silicon Composite Film

doi:10.1007/s40242-019-8331-2

高等学校化学研究 ›› 2019, Vol. 35 ›› Issue (2): 193-199.doi: 10.1007/s40242-019-8331-2

Detection of Amines in Lamb Spoilage by Optical Waveguide Sensor Based on Bromophenol Blue-Silicon Composite Film

KOXMAK Sayyara¹, YIMAMUMAIMAITI Tajiguli², ABDUKEREMU Hannikezi¹, NIZAMIDIN Patima¹, YIMIT Abliz¹

1. College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, P. R. China;
2. State Key Laboratory of Analytical Chemistry for Life Science, Collaborative Innovation of Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, P. R. China

收稿日期:2018-10-15 修回日期:2018-12-17 出版日期:2019-04-01 发布日期:2019-04-30
通讯作者: YIMIT Abliz E-mail:ablizyimit@xju.edu.cn
基金资助:
Supported by the National Natural Science Foundation of China(No.21765021).

Detection of Amines in Lamb Spoilage by Optical Waveguide Sensor Based on Bromophenol Blue-Silicon Composite Film

KOXMAK Sayyara¹, YIMAMUMAIMAITI Tajiguli², ABDUKEREMU Hannikezi¹, NIZAMIDIN Patima¹, YIMIT Abliz¹

1. College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, P. R. China;
2. State Key Laboratory of Analytical Chemistry for Life Science, Collaborative Innovation of Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, P. R. China

Received:2018-10-15 Revised:2018-12-17 Online:2019-04-01 Published:2019-04-30
Contact: YIMIT Abliz E-mail:ablizyimit@xju.edu.cn
Supported by:
Supported by the National Natural Science Foundation of China(No.21765021).

摘要/Abstract

摘要： We herein report the development of a bromophenol blue(BPB)-silicone composite film/K⁺-exchange glass optical waveguide(OWG) sensor for the detection of amines produced during the spoilage of lamb. The optical and structural properties of the sensitive thin film were studied by ultraviolet-visible(UV-Vis) spectroscopy, and the light source of the OWG detecting system was selected. Gas sensing measurements showed that the sensor exhibited a good selectivity, high sensitivity, and short response-recovery time towards volatile amine gases in the 0.00117-11.72 mg/g range. The as-prepared optical waveguide device was subsequently applied in the determination of gases (namely trimethylamine, dimethylamine, and ammonia) emitted from the lamb samples(5 g) stored at room temperature(25℃) and in a refrigerator(5℃) for 0-4 d, and the total volatile basic nitrogen(TVB-N) contents were detected by UV-Vis spectroscopy, and the results were compared with those obtained using our detector. It was found that the sensing element was capable of detecting mixed gases produced by the decomposition of lamb samples in a refrigerator for 0.5 h, where the TVB-N content was lower than 35 μg/g.

关键词: Optical waveguide sensor, Composite film, Amine gas, Lamb freshness detection

Abstract: We herein report the development of a bromophenol blue(BPB)-silicone composite film/K⁺-exchange glass optical waveguide(OWG) sensor for the detection of amines produced during the spoilage of lamb. The optical and structural properties of the sensitive thin film were studied by ultraviolet-visible(UV-Vis) spectroscopy, and the light source of the OWG detecting system was selected. Gas sensing measurements showed that the sensor exhibited a good selectivity, high sensitivity, and short response-recovery time towards volatile amine gases in the 0.00117-11.72 mg/g range. The as-prepared optical waveguide device was subsequently applied in the determination of gases (namely trimethylamine, dimethylamine, and ammonia) emitted from the lamb samples(5 g) stored at room temperature(25℃) and in a refrigerator(5℃) for 0-4 d, and the total volatile basic nitrogen(TVB-N) contents were detected by UV-Vis spectroscopy, and the results were compared with those obtained using our detector. It was found that the sensing element was capable of detecting mixed gases produced by the decomposition of lamb samples in a refrigerator for 0.5 h, where the TVB-N content was lower than 35 μg/g.

Key words: Optical waveguide sensor, Composite film, Amine gas, Lamb freshness detection

KOXMAK Sayyara, YIMAMUMAIMAITI Tajiguli, ABDUKEREMU Hannikezi, NIZAMIDIN Patima, YIMIT Abliz. Detection of Amines in Lamb Spoilage by Optical Waveguide Sensor Based on Bromophenol Blue-Silicon Composite Film[J]. 高等学校化学研究, 2019, 35(2): 193-199.

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Detection of Amines in Lamb Spoilage by Optical Waveguide Sensor Based on Bromophenol Blue-Silicon Composite Film

Detection of Amines in Lamb Spoilage by Optical Waveguide Sensor Based on Bromophenol Blue-Silicon Composite Film

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