Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative

高等学校化学研究 ›› 2011, Vol. 27 ›› Issue (4): 574-577.

Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative

QIAO Yan-hong¹, LIN Hai³ and LIN Hua-kuan^2*

1. Department of Chemistry, Tianjin Normal University, Tianjin 300387, P. R. China;
2. Department of Chemistry, Nankai University, Tianjin 300071, P. R. China;
3. Key Laboratory of Functional Polymer Materials, Ministry of Education, Nankai University, Tianjin 300070, P. R. China

收稿日期:2010-08-20 修回日期:2011-03-28 出版日期:2011-07-25 发布日期:2011-06-29
通讯作者: LIN Hua-kuan E-mail:hklin@nankai.edu.cn
基金资助:
Supported by the National Natural Science Foundation of China(Nos.20371028, 20671052) and the Doctor Foundation of Tianjin Normal University, China(No.52LX31).

Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative

QIAO Yan-hong¹, LIN Hai³ and LIN Hua-kuan^2*

1. Department of Chemistry, Tianjin Normal University, Tianjin 300387, P. R. China;
2. Department of Chemistry, Nankai University, Tianjin 300071, P. R. China;
3. Key Laboratory of Functional Polymer Materials, Ministry of Education, Nankai University, Tianjin 300070, P. R. China

Received:2010-08-20 Revised:2011-03-28 Online:2011-07-25 Published:2011-06-29
Contact: LIN Hua-kuan E-mail:hklin@nankai.edu.cn
Supported by:
Supported by the National Natural Science Foundation of China(Nos.20371028, 20671052) and the Doctor Foundation of Tianjin Normal University, China(No.52LX31).

摘要/Abstract

摘要： A simple colorimetric acetate ion receptor based on 3-methoxysalicylaldehyde-4′-nitrophenyl-hydrazone was synthesized in an ethanol solution through one step, and characterized by 1H NMR and elemental analyses. Its anion-binding ability was examined by UV-Vis absorption spectroscopy in DMSO(dimethyl sulfoxide). The result shows that the compound has a high affinity for and a high selectivity toward acetate ions, and also an advantage of ‘naked-eye’ recognition of color changing from yellow to purple.

关键词: Anion recognition, Colorimetric, ‘Naked-eye&rsquo, recognition, Schiff base

Abstract: A simple colorimetric acetate ion receptor based on 3-methoxysalicylaldehyde-4′-nitrophenyl-hydrazone was synthesized in an ethanol solution through one step, and characterized by 1H NMR and elemental analyses. Its anion-binding ability was examined by UV-Vis absorption spectroscopy in DMSO(dimethyl sulfoxide). The result shows that the compound has a high affinity for and a high selectivity toward acetate ions, and also an advantage of ‘naked-eye’ recognition of color changing from yellow to purple.

Key words: Anion recognition, Colorimetric, ‘Naked-eye&rsquo, recognition, Schiff base

QIAO Yan-hong, LIN Hai and LIN Hua-kuan*. Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative[J]. 高等学校化学研究, 2011, 27(4): 574-577.

QIAO Yan-hong, LIN Hai and LIN Hua-kuan*. Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative[J]. Chemical Research in Chinese Universities, 2011, 27(4): 574-577.

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Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative

Design, Synthesis and Recognition Properties of a New Acetate Ion Receptor Based on Shiff-base Derivative

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