Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction

doi:10.1007/s40242-015-4364-3

高等学校化学研究 ›› 2015, Vol. 31 ›› Issue (3): 352-356.doi: 10.1007/s40242-015-4364-3

Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction

ZHAO Zhenying¹, LIN Jun¹, YU Yong¹, HOU Chuanbin², SUN Yuyang¹

1. College of Instrumentation & Electrical Engineering, Jilin University, Changchun 130061, P. R. China;
2. College of Construction Engineering, Jilin University, Changchun 130061, P. R. China

收稿日期:2014-09-29 修回日期:2015-02-16 出版日期:2015-06-01 发布日期:2015-03-30
通讯作者: LIN Jun E-mail:lin_jun@jlu.edu.cn
基金资助:
Supported by the National Innovation Project of Production-Study-Research-Application of China(No.OSR-02-04), the Research Fund for the Doctoral Program of Higher Education of China(No.20130061110068) and the National Natural Science Foundation of China(No.21207047).

Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction

ZHAO Zhenying¹, LIN Jun¹, YU Yong¹, HOU Chuanbin², SUN Yuyang¹

1. College of Instrumentation & Electrical Engineering, Jilin University, Changchun 130061, P. R. China;
2. College of Construction Engineering, Jilin University, Changchun 130061, P. R. China

Received:2014-09-29 Revised:2015-02-16 Online:2015-06-01 Published:2015-03-30
Contact: LIN Jun E-mail:lin_jun@jlu.edu.cn
Supported by:
Supported by the National Innovation Project of Production-Study-Research-Application of China(No.OSR-02-04), the Research Fund for the Doctoral Program of Higher Education of China(No.20130061110068) and the National Natural Science Foundation of China(No.21207047).

摘要/Abstract

摘要：

The oil yield of oil shale was evaluated by Fourier transform infrared(FTIR) spectrometry coupled with ultrasound-assisted extraction. The extraction conditions, including the amount of sample, extraction time and extraction temperature, were examined and optimized. Twenty-four oil shale samples were collected and divided into calibration set and prediction set randomly with a ratio of 2:1. The oil yields of all the samples were determined by the routine method(low-temperature retorting) for reference. The linear regression(LR) equations of oil yield vs. the total area of the spectrum peaks in a wavenumber range of 3100-2800 cm^-1 as well as the sum of absorbance of three absorption peaks(2855, 2927 and 2955 cm^-1), and the multiple linear regression(MLR) model of oil yield vs. the absorbances of the three absorption peaks were constructed with the samples in calibration set and applied to the evaluation of the oil yields of the samples in prediction set, respectively. The results show that the MLR model provides more accurate predictions than the other LR two equations. The determination coefficient(R_p²), the root-mean-square error of prediction(RMSEP) and the residual prediction deviation(RPD) of the MLR model are 0.9616, 0.6458 and 3.6, respectively. The present method is a rapid and effective alternative to the routine low-temperature retorting method.

关键词: Oil shale, Oil yield, Ultrasound-assisted extraction, Infrared spectroscopy, Multiple linear regression

Abstract:

Key words: Oil shale, Oil yield, Ultrasound-assisted extraction, Infrared spectroscopy, Multiple linear regression

ZHAO Zhenying, LIN Jun, YU Yong, HOU Chuanbin, SUN Yuyang. Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction[J]. 高等学校化学研究, 2015, 31(3): 352-356.

ZHAO Zhenying, LIN Jun, YU Yong, HOU Chuanbin, SUN Yuyang. Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction[J]. Chemical Research in Chinese Universities, 2015, 31(3): 352-356.

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Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction

Evaluation of Oil Yield of Oil Shale by Infrared Spectrometry Coupled with Ultrasound-assisted Extraction

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