Structural Characterization and Luminescence Properties of Two 4d-4f Ln-Ag Coordination Compounds Based on Dinuclear Lanthanide Clusters

doi:10.1007/s40242-014-3368-8

高等学校化学研究 ›› 2014, Vol. 30 ›› Issue (2): 194-199.doi: 10.1007/s40242-014-3368-8

Structural Characterization and Luminescence Properties of Two 4d-4f Ln-Ag Coordination Compounds Based on Dinuclear Lanthanide Clusters

ZHANG Yu, CHEN Lei, JU Weiwei, XU Yan

State Key Laboratory of Materials-oriented Chemical Engineering, College of Chemistry and Chemical Engineering, Nanjing Tech University, Nanjing 210009, P. R. China

收稿日期:2013-08-30 修回日期:2013-10-24 出版日期:2014-04-01 发布日期:2013-11-05
通讯作者: XU Yan E-mail:yanxu@njtech.edu.cn
基金资助:
Supported by the Natural Science Foundation of Jiangsu Province, China(No.BK2012823) and the Project of Priority Academic Program Development of Jiangsu Higher Education Institutions, China.

Structural Characterization and Luminescence Properties of Two 4d-4f Ln-Ag Coordination Compounds Based on Dinuclear Lanthanide Clusters

ZHANG Yu, CHEN Lei, JU Weiwei, XU Yan

State Key Laboratory of Materials-oriented Chemical Engineering, College of Chemistry and Chemical Engineering, Nanjing Tech University, Nanjing 210009, P. R. China

Received:2013-08-30 Revised:2013-10-24 Online:2014-04-01 Published:2013-11-05
Contact: XU Yan E-mail:yanxu@njtech.edu.cn
Supported by:
Supported by the Natural Science Foundation of Jiangsu Province, China(No.BK2012823) and the Project of Priority Academic Program Development of Jiangsu Higher Education Institutions, China.

摘要/Abstract

摘要：

Two new compounds,[ErAg(INA)₂(C₂O₄)]·2H₂O(1)(HINA=nicotinic acid) and [Tb_0.8Y_0.2Ag₂(IN)₄·(H₂O)₅]·NO₃·2H₂O(2)(HIN=isonicotinic acid), based on the {Ln₂} building units, have been hydrothermally synthesized and characterized by single-crystal X-ray diffraction, infrared spectroscopy, thermal analysis and powder X-ray diffraction(PXRD). Single-crystal X-ray diffraction data reveal that both compounds crystallized in the low-symmetry triclinic space group P1. Compound 1 is a 3D heterometallic coordination framework based on {Er₂} clusters, oxalate ligands and bridging [Ag(INA)] linkers, while compound 2 consists of 0D [Tb_0.8·Y_0.2Ag₂(IN)₄(H₂O)₅]₂ subunits that give a 3D supramolecular structure through hydrogen bond interaction. The photoluminescent properties of both compounds(1 and 2) were studied.

关键词: 4d-4f Ln-Ag coordination compound, Doping, Hydrothermal synthesis, Crystal structure

Abstract:

Key words: 4d-4f Ln-Ag coordination compound, Doping, Hydrothermal synthesis, Crystal structure

ZHANG Yu, CHEN Lei, JU Weiwei, XU Yan. Structural Characterization and Luminescence Properties of Two 4d-4f Ln-Ag Coordination Compounds Based on Dinuclear Lanthanide Clusters[J]. 高等学校化学研究, 2014, 30(2): 194-199.

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Structural Characterization and Luminescence Properties of Two 4d-4f Ln-Ag Coordination Compounds Based on Dinuclear Lanthanide Clusters

Structural Characterization and Luminescence Properties of Two 4d-4f Ln-Ag Coordination Compounds Based on Dinuclear Lanthanide Clusters

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