高等学校化学研究 ›› 1989, Vol. 5 ›› Issue (2): 138-146.
The Reactions of 1-Acetothiosemicarbazidc with P（NR2）3 PC13 and PCI5
Zhang Jingling, Xu Wei
- Institute of Organic Synthesis, Huazhong Aormal University, Wuhan
The Reactions of 1-Acetothiosemicarbazidc with P（NR2）3 PC13 and PCI5
Zhang Jingling, Xu Wei
- Institute of Organic Synthesis, Huazhong Aormal University, Wuhan
摘要： A Series of new heterocyciophosphorus compounds were synthesizec oy cyclocondensa-tion of 1-acetothiosemicarbazide with P(NR2)3.The further reaction of these compounds with P(NR2)3 gave different compounds depending upon different reaction conditions.The 1-acetothiosemicarbazide can also condense with PCl3 and PCl5 similarly, The reaction mechanism, the spectral properties and chemical properties of these products were also studied and discussed.