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高等学校化学研究 ›› 2006, Vol. 22 ›› Issue (3): 297-301.

• Articles • 上一篇    下一篇

Evaluation of Improved Ultrasonic Nebulizer for Miniature Simultaneous Microwave Plasma Torch Spectrometer

FENG Guo-dong, JIANG Jie, HUAN Yan-fu, ZHENG Jian, LI Ming, CAO Yan-bo, JIN Qin-han, YU Ai-min   

  1. Department of Analytical Chemistry, College of Chemistry, Jilin University, Changchun 130021, P. R. China
  • 收稿日期:2005-02-28 出版日期:2006-06-24 发布日期:2011-08-06
  • 基金资助:

    Supported by the Key Project for Science and Technology Development, Jilin Province, China(No. 20010306-1).

Evaluation of Improved Ultrasonic Nebulizer for Miniature Simultaneous Microwave Plasma Torch Spectrometer

FENG Guo-dong, JIANG Jie, HUAN Yan-fu, ZHENG Jian, LI Ming, CAO Yan-bo, JIN Qin-han, YU Ai-min   

  1. Department of Analytical Chemistry, College of Chemistry, Jilin University, Changchun 130021, P. R. China
  • Received:2005-02-28 Online:2006-06-24 Published:2011-08-06
  • Supported by:

    Supported by the Key Project for Science and Technology Development, Jilin Province, China(No. 20010306-1).

摘要: A new automatic sample solution introduction system for miniature simultaneous microwave plasma torch(MPT)atomic emission spectrometer was developed. The operating parameters were optimized. The detection limits of the spectrometer with an ultrasonic nebulizer for Ag, Al, Ba, Ca, Cr, Cu, Fe, Mg, Mn, Sr, and V are 5-10 times lower than those obtained with a pneumatic nebulizer and are also lower than those obtained by a Model JX-1010 MPT spectrometer. Two practical samples were analyzed to test the reliability and sensitivity of the system.

关键词: Microwave plasma torch, Miniature simultaneous spectrometer, Ultrasonic nebulizer, Automatic introduction system

Abstract: A new automatic sample solution introduction system for miniature simultaneous microwave plasma torch(MPT)atomic emission spectrometer was developed. The operating parameters were optimized. The detection limits of the spectrometer with an ultrasonic nebulizer for Ag, Al, Ba, Ca, Cr, Cu, Fe, Mg, Mn, Sr, and V are 5-10 times lower than those obtained with a pneumatic nebulizer and are also lower than those obtained by a Model JX-1010 MPT spectrometer. Two practical samples were analyzed to test the reliability and sensitivity of the system.

Key words: Microwave plasma torch, Miniature simultaneous spectrometer, Ultrasonic nebulizer, Automatic introduction system